Acid neutralizing is a big problem with vacuum pumps. We see a lot
of pumps and talk to a lot of people with problems in this area. Many
acids can be pumped because they go into a gas phase (become a vapor) when
hit with a high vacuum. Often the customer wants the acid out of the
product they are pulling a vacuum on but they do not realize this acid
then goes somewhere. A lot of times it goes into the vacuum
pump. This main issue can be dealt with a couple of different
ways.
First and foremost we want to stop the acid from moving into the pump
if at all possible. For this we generally use a trap.
What's going on here?
The customer needs to detail the chemicals or contaminants in the
system that will be pumped or that have a "low vapor
pressure". A list should be made of the items to be placed
under vacuum and the vapor pressure of each item detailed on a
sheet. Understanding at what pressure an item comes across can make
understanding quantitatively (actual amount) the amount of each chemical
item present. You can even get an idea of pump down time based on
sample size once this is known. Use of a good vacuum gauge depending
on chemicals pumped can greatly assist in this effort and help create the
detail. The pump will pump a given chemical at a specific vapor
pressure until it is removed from the sample by turning it into a
gas. After the first item is turned into a gas and pumped then the
evacuation process moves onto the next item on the list with the next
lower vapor pressure. Timing this whole sequence can be rather
enlightening and also helps us review our basic physical chemistry
skills. Remember PV=nRT? Well this is what is happening
here. Just as a real simple example say we had a milliliter of nice
fresh Pepsi-cola. Hit it with a vacuum and first all the CO2 will be
pumped (removes the fizz) then we would pump the water out of the sample
and be left with only sugar, caramel color (assuming we stopped after the
water) and whatever other secret ingredients might be in there with a
vapor pressure point greater than water.
Get back to the point.
Ok, understanding vapor pressure points and all and knowing that we can
pump acids and understanding these are bad for your pump what the heck do
we do now? Stop these bad actors from getting in the pump.
Generally we "trap" them. This can happen typically using
a cold trap. This cold trap deal is addressed in more detail
elsewhere. We can also to a degree, neutralize them by moving them
through a trap with a "base" product in the trap. Back to
chemistry class again ACID+BASE= Salt + Water. I know I have overly
simplified this for many of you, but it works in principle. Our VIT
traps have an option for a Acid Neut Element. This element employs
KOH or Potassium Hydroxide in the element. This product is highly
basic. As the acid vapors hit the element the convert to the acid
salt and water. This is not perfect again but at least it helps in
stopping the bad actors from just marching into the pump. The trap
is a help and really should be used after a decent cold trap. The trap has
a blue indicator as part of it's makeup to tell when it has been used up
and should be replaced.
Some customers state that the pump runs, but if they shut it down with
acid rich oil then it locks up or is tough to get going again. If
your system is contaminated, keep the pump running until you can change
the oil. HyVac pumps are designed to run for extended periods of
time days, weeks, months on end (although not with contaminated
oil). But if your pump has been used for a nasty process valve it
off and keep it running and arrange to change the oil as soon as possible.
Change the OIL OFTEN. Unfortunately you have a tough
system and are going to have to watch you oil quality on a regular
basis. Nothing really substitutes for this task. Sorry,
but it is part of your process that must be dealt with. If you do
not want to maintain it, understandable, get someone to do it for you or
you will be sending your expensive vacuum pump to us for expensive
repairs. We really don't mind this, it helps us stay in business,
but we are trying to help you save some money, downtime and aggravation
here.
see also cold traps,
changing the oil and water in the
pump.
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